Publications in peer-reviewed journals:

Yiannis Fiamegos, Sergej Papoci, Catalina Dumitrascu, Michele Ghidotti, Tereza Zdiniakova, Franz Ulberth and María Beatriz de la Calle Guntiñas. Are the elemental fingerprints of organic and conventional food different? ED-XRF as screening technique. Journal of Food Composition and Analysis, 99, 103854, (2021). https://doi.org/10.1016/j.jfca.2021.103854 

Yiannis Fiamegos , Catalina Dumitrascu , Maria Beatriz de la Calle, “Authentication of PDO paprika powder (Pimentón de la Vera) by multivariate analysis of the elemental fingerprint determined by ED-XRF”, Food Control, 120, 107496, (2021). https://doi.org/10.1016/j.foodcont.2020.107496. 

Michele Ghidotti, Yiannis Fiamegos, Catalina Dumitrascu and María Beatriz de la Calle Guntiñas, “Use of elemental profiles to verify geographical origin and botanical variety of Spanish honeys with a Protected Denomination of Origin”, Food Chemistry, 342, 128350, (2021). https://doi.org/10.1016/j.foodchem.2020.128350.

Catalina Dumitrascu, Yiannis Fiamegos, Maria Beatriz de la Calle Guntiñas. Feasibility study on the use of elemental profiles to authenticate aromatic rice: the case of Basmati and Thai rice. Analytical and Bioanalytical Chemistry, 413(20), 4947-4957, (2021), (https://doi.org/10.1007/s00216-021-03455-9).

Michele Ghidotti, Sergej Papoci, Catalina Dumitrascu, Tereza Zdiniakova, Yiannis Fiamegos, María Beatriz de la Calle Guntiñas. ED-XRF as screening tool to help custom laboratories in their fight against fraud. Talanta, 3, 100040, (2021).  (https://doi.org/10.1016/j.talo.2021.100040).

Yiannis Fiamegos, Catalina Dumitrascu, Michele Ghidotti and Maria Beatriz de la Calle Guntiñas, “Use of Energy Dispersive-X Ray Fluorescence combined with chemometrics modelling to classify honey according to botanical variety and geographical origin”, Analytical and Bioanalytical Chemistry, 412(2), 463-472, (2020). https://doi.org/10.1007/s00216-019-02255-6 

Tereza Zdiniakova, María Beatriz de la Calle, “Feasibility study about the use of element profiles determined by ED XRF as screening method to authenticate coconut sugar commercially available”, European Food Research and Technology, 246, 2101-2109, (2020). https://doi.org/10.1007/s00217-020-03559-z 

Ballin, N.Z., Omar Onaindia, J., Jawad, H., Fernandez-Carazo, R., Maquet, A.(2019) High-resolution melting of multiple barcode amplicons for plant species authentication. Food Control 105, 141-150.

Paracchini, V., Petrillo, M., Lievens, A., Kagkli, D.-M., Angers-Loustau, A. (2019) Nuclear DNA barcodes for cod identification in mildly-treated and processed food products. Food Additives and Contaminants - Part A 36, 1-14

Conte, L., Bendini, A., Valli, E.,   Lucci, P., Moret, S., Maquet, A., Lacoste, F., Brereton, P., García-González, D.L., Moreda, W., Gallina Toschi, T. (2019) Olive oil quality and authenticity: A review of current EU legislation, standards, relevant methods of analyses, their drawbacks and recommendations for the future. Trends in Food Science and Technology, in press

Cubero-Leon, E., De Rudder, O., Maquet, A. (2018) Metabolomics for organic food authentication: Results from a long-term field study in carrots. Food Chemistry 239, 760-770

Paracchini, V., Petrillo, M., Lievens, A., Puertas Gallardo, A., Martinsohn, J.T., Hofherr, J., Maquet, Silva, A.P.B., Kagkli, D.M., Querci, M., Patak, A., Angers-Loustau, A. (2017) Novel nuclear barcode regions for the identification of flatfish species. Food Control 79, 297-308

Lehto, S., Buchweitz, M., Klimm, A., Straßburger, R., Bechtold, C., Ulberth, F. (2017) Comparison of food colour regulations in the EU and the US: a review of current provisions. Food Additives and Contaminants - Part A 34, pp. 335-355

Omar, J., Slowikowski, B., Boix, A., von Holst, C. (2017) Spectroscopy applied to feed additives of the European Union Reference Laboratory: a valuable tool for traceability. Food Additives and Contaminants - Part A 34, 1272-1284

Ortea, I., O'Connor, G., Maquet, A. (2016) Review on proteomics for food authentication. Journal of Proteomics 147, 212-225

Angers-Loustau, A., Petrillo, M., Paracchini, V., Kagkli, D.M., Rischitor, P.E.,  Puertas Gallardo, A. Patak, A., Querci, M., Kreysa, J.  (2016) Towards plant species identification in complex samples: A bioinformatics pipeline for the identification of novel nuclear barcode candidates. PLoS ONE 11, e0147692

de Jong, J., López, P., Mol, H., Baeten, V., Fernández Pierna, J.A., Vermeulen, P., Vincent, U., Boix, A., von Holst, C., Tomaniova, M., Hajslova, J., Yang, Z., Han, L., MacDonald, S., Haughey, S.A., Elliott, C.T. (2016) Analytical strategies for the early quality and safety assurance in the global feed chain. Approaches for nitrogen adulterants in soybean meal and mineral and transformer oils in vegetable oils. TrAC - Trends in Analytical Chemistry 76, 203-215

Ulberth, F. (2016) Early warning systems for food safety and integrity need to be anticipative to be useful for preventing food crisis situations. Journal für Verbraucherschutz und Lebensmittelsicherheit 11, 215-216

Tena, N., Boix, A., von Holst, C. (2015) Identification of botanical and geographical origin of distillers dried grains with solubles by near infrared microscopy. Food Control 54, 103-110

Vermeulen, P., Nietner, T., Haughey, S.A., Yang, Z., Tena, N., Chmelarova, H., Van Ruth, S., Tomaniova, M., Boix, A., Han, L., Elliott, C.T., Baeten, V., Fauhl-Hassek, C. (2015) Origin authentication of distillers' dried grains and solubles (DDGS) - Application and comparison of different analytical strategies. Analytical and Bioanalytical Chemistry 407, 6447-6461

Alonso-Salces, R.M., Segebarth, N., Garmón-Lobato, S., Holland, M.V., Moreno-Rojas, J.M., Fernández-Pierna, J.A., Baeten, V., Fuselli, S.R., Gallo, B, Berrueta, L.A., Reniero, F., Guillou, C., Héberger, K. (2015) 1 H-NMR and isotopic fingerprinting of olive oil and its unsaponifiable fraction: Geographical origin of virgin olive oils by pattern recognition. European Journal of Lipid Science and Technology 117, 1991-2006

Cubero-Leon, E., Peñalver, R., Maquet, A. (2014) Review on metabolomics for food authentication. Food Research International 60, 95-107

Tena, N., Fernández Pierna, J.A., Boix, A., Baeten, V., von Holst, C. (2014) Differentiation of meat and bone meal from fishmeal by near-infrared spectroscopy: Extension of scope to defatted samples. Food Control 43, 155-162

Prado, M., Boix, A., von Holst, C. (2013) Development of a real-time PCR method for the simultaneous detection of mackerel and horse mackerel. Food Control 34, pp. 19-23, link

Camin, F., Bontempo, L., Perini, M., Tonon, A., Breas, O., Guillou, C., Moreno-Rojas, J.M., Moreno-Rojas, J.M., Gagliano, G. (2013) Control of wine vinegar authenticity through δ 18O analysis. Food Control 29, 107-111

Tenea, G.N., Cordeiro Raposo, F., Maquet, A. (2012) Comparative transcriptome profiling in winter wheat grown under different agricultural practices.  Journal of Agricultural and Food Chemistry 60, 10970-10978

Prado, M., Boix, A., Von Holst, C. (2012) Novel approach for the simultaneous detection of DNA from different fish species based on a nuclear: Quantification potential. Analytical and Bioanalytical Chemistry 403, 3041-3050

Voerkelius, S., Lorenz, G.D., Rummel, S., Quétel, C.R., Heiss, G., Baxter, M., Brach-Papa, C., Deters-Itzelsberger, P., Hoelzl, S., Hoogewerff, J., Ponzevera, E., Van Bocxstaele, M., Ueckermann, H. (2010) Strontium isotopic signatures of natural mineral waters, the reference to a simple geological map and its potential for authentication of food. Food Chemistry 118, 933-940

Tenea, G.N., Peres Bota, A., Cordeiro Raposo, F., Maquet, A. (2011)  Reference genes for gene expression studies in wheat flag leaves grown under different farming conditions. BMC Research Notes 4, 373

Lindahl, P., Maquet, A., Hult, M., Gasparro, J., Marissens, G., González de Orduña, R. (2011) Natural radioactivity in winter wheat from organic and conventional agricultural systems. Journal of Environmental Radioactivity 102, 163-169

Alonso-Salces, R.M., Holland, M.V., Guillou, C. (2011) 1H-NMR fingerprinting to evaluate the stability of olive oil.  Food Control 22, 2041-2046

Mattarucchi, E., Stocchero, M., Moreno-Rojas, J.M., Giordano, G., Reniero, F., Guillou, C. (2010) Authentication of trappist beers by LC-MS fingerprints and multivariate data analysis. Journal of Agricultural and Food Chemistry 58, 12089-12095

Aramendía, M.A., Marinas, A., Marinas, J.M., Sánchez, E., Urbano, F.J., Guillou, C., Moreno Rojas, J.M., Moalem, M., Rallo, L. (2010) A nuclear magnetic resonance (1H and 13C) and isotope ratio mass spectrometry (δ13C, δ2H and δ18O) study of andalusian olive oils. Rapid Communications in Mass Spectrometry 24, 1457-1466

Alonso-Salces, R.M., Moreno-Rojas, J.M., Holland, M.V., Reniero, F., Guillou, C., Héberger, K. (2010) Virgin olive oil authentication by multivariate analyses of 1H NMR fingerprints and γ13c and γ2h data. Journal of Agricultural and Food Chemistry 58, 5586-5596

Alonso-Salces, R.M., Héberger, K., Holland, M.V., Moreno-Rojas, J.M., Mariani, C., Bellan, G., Reniero, F., Guillou, C. (2010) Multivariate analysis of NMR fingerprint of the unsaponifiable fraction of virgin olive oils for authentication purposes. Food Chemistry 118, 956-965

Szulc, M., Maquet, A. (2009) Extraction protocol for winter wheat whole grain proteins compatible with two-dimensional fluorescence difference gel electrophoresis (2D DIGE). Cereal Chemistry 86,  692-694

Maçatelli, M., Akkermans, W., Koot, A., Buchgraber, M., Paterson, A., van Ruth, S. (2009) Verification of the geographical origin of European butters using PTR-MS. Journal of Food Composition and Analysis 22, 169-175

Mannina, L., D'Imperio, M., Capitani, D., Rezzi, S., Guillou, C., Mavromoustakos, T., Vilchez, M.D.M., Fernández, A.H., Thomas, F., Aparicio, R. (2009) 1H NMR-based protocol for the detection of adulterations of refined olive oil with refined hazelnut oil. Journal of Agricultural and Food Chemistry 57, 11550-11556

Moreno-Rojas, J.M., Tulli, F., Messina, M., Tibaldi, E., Guillou, C. (2008) Stable isotope ratio analysis as a tool to discriminate between rainbow trout (O. mykiss) fed diets based on plant or fish-meal proteins. Rapid Communications in Mass Spectrometry 22, 3706-3710 

Moreno-Rojas, J.M., Vasta, V., Lanza, A., Luciano, G., Ladroue, V., Guillou, C., Priolo, A. (2008) Stable isotopes to discriminate lambs fed herbage or concentrate both obtained from C3 plants. Rapid Communications in Mass Spectrometry 22, 3701-3705    

Araghipour, N., Colineau, J., Koot, A., Akkermans, W., Rojas, J.M.M., Beauchamp, J., Wisthaler, A., Märk, T.D., Downey, G., Guillou, C., Mannina, L., van Ruth, S. (2008) Geographical origin classification of olive oils by PTR-MS. Food Chemistry 108, 374-383

Busetto, M.L., Moretti, V.M., Moreno-Rojas, J.M., Caprino, F., Giani, I., Malandra, R., Bellagamba, F., Guillou, C. (2008) Authentication of farmed and wild turbot (Psetta maxima) by fatty acid and isotopic analyses combined with chemometrics. Journal of Agricultural and Food Chemistry 56, 2742-2750

Calderone, G., Guillou, C. (2008) Analysis of isotopic ratios for the detection of illegal watering of beverages. Food Chemistry 106, 1399-1405

Thomas, F., Jamin, E., Wietzerbin, K., Guérin, R., Lees, M., Morvan, E., Billault, I., Derrien, S., Rojas, J.M.M., Serra, F., Guillou, C., Aursand, M., McEvoy, L., Prael, A., Robin, R.J. (2008) Determination of origin of atlantic salmon (Salmo salar): The use of multiprobe and multielement isotopic analyses in combination with fatty acid composition to assess wild or farmed origin. Journal of Agricultural and Food Chemistry 56, 989-997

Rezzi, S., Giani, I., Héberger, K., Axelson, D.E., Moretti, V.M., Reniero, F., Guillou, C. (2007) Classification of gilthead sea bream (Sparus aurata) from 1H NMR lipid profiling combined with principal component and linear discriminant analysis. Journal of Agricultural and Food Chemistry 55, 9963-9968

Moreno Rojas, J.M., Cosofret, S., Reniero, F., Guillou, C., Serra, F.  (2007) Control of oenological products: Discrimination between different botanical sources of L-tartaric acid by isotope ratio mass spectrometry. Rapid Communications in Mass Spectrometry 21, 2447-2450

Calderone, G., Guillou, C., Reniero, F., Naulet, N. (2007) Helping to authenticate sparkling drinks with 13C/12C of CO2 by gas chromatography-isotope ratio mass spectrometry. Food Research International 40, 324-331

Bréas, O., Thomas, F., Zeleny, R., Calderone, G., Jamin, E., Guillou, C. (2007) Performance evaluation of elemental analysis/isotope ratio mass spectrometry methods for the determination of the D/H ratio in tetramethylurea and other compounds - Results of a laboratory inter-comparison. Rapid Communications in Mass Spectrometry 21, 1555-1560

Moreno Rojas, J.M., Serra, F., Giani, I., Moretti, V.M., Reniero, F., Guillou, C. (2007) The use of stable isotope ratio analyses to discriminate wild and farmed gilthead sea bream (Sparus aurata).  Rapid Communications in Mass Spectrometry 21, 207-211

Masoum, S., Malabat, C., Jalali-Heravi, M., Guillou, C., Rezzi, S., Rutledge, D.N. (2007) Application of support vector machines to 1H NMR data of fish oils: Methodology for the confirmation of wild and farmed salmon and their origins. Analytical and Bioanalytical Chemistry 387, 1499-1510

Buchgraber, M., Androni, S., Berndt, E.-M., Kaufmann-Horlacher, I., Lomnitz, A., Matissek, R., Maurer, R., Neuberger, G., Rodriguez-Estrada, M.T., Schreiner, M., Schulokat, S., Schut, M., Wachter, N. (2007) Gas-liquid chromatographic determination of milk fat and cocoa butter equivalents in milk chocolate: Interlaboratory study. Journal of AOAC International 90, 1326-1339

Buchgraber, M., Androni, S., Anklam, E. (2007) Quantification of milk fat in chocolate fats by triacylglycerol analysis using gas-liquid chromatography. Journal of Agricultural and Food Chemistry 55, 3275-3283

Buchgraber, M., Androni, S., Anklam, E. (2007) Determination of cocoa butter equivalents in milk chocolate by triacylglycerol profiling. Journal of Agricultural and Food Chemistry 55, 3284-3291

Rezzi, S., Axelson, D.E., Héberger, K., Reniero, F., Mariani, C., Guillou, C. (2005) Classification of olive oils using high throughput flow 1H NMR fingerprinting with principal component analysis, linear discriminant analysis and probabilistic neural networks. Analytica Chimica Acta 552, 13-24

Serra, F., Guillou, C.G., Reniero, F., Ballarin, L., Cantagallo, M.I., Wieser, M., Iyer, S.S., Héberger, K., Vanhaecke, F. (2005) Determination of the geographical origin of green coffee by principal component analysis of carbon, nitrogen and boron stable isotope ratios. Rapid Communications in Mass Spectrometry 19, 2111-2115

Serra, F., Reniero, F., Guillou, C.G., Moreno, J.M., Marinas, J.M., Vanhaecke, F. (2005) 13C and 18O isotopic analysis to determine the origin of L-tartaric acid. Rapid Communications in Mass Spectrometry 19, 1227-1230

Calderone, G., Naulet, N., Guillou, C., Reniero, F., Cortes, A.I.B. (2005) Analysis of the 13C natural abundance of CO2 gas from sparkling drinks by gas chromatography/combustion/isotope ratio mass spectrometry. Rapid Communications in Mass Spectrometry 19, 701-705

Siderer, Y., Maquet, A., Anklam, E. (2005) Need for research to support consumer confidence in the growing organic food market. Trends in Food Science and Technology 16, 332-343 

Calderone, G., Naulet, N., Guillou, C., Reniero, F. (2004) Characterization of European wine glycerol: Stable carbon isotope approach. Journal of Agricultural and Food Chemistry 52, 5902-5906

Fauhl, C., Wittkowski, R., Lofthouse, J., Hird, S., Brereton, P., Versini, G., Lees, M., Guillou, C. (2004) Gas chromatographic/mass spectrometric determination of 3-methoxy-1,2-propanediol and cyclic diglycerols, by-products of technical glycerol, in wine: Interlaboratory study. Journal of AOAC International 87, 1179-1188

Buchgraber, M., Ulberth, F., Anklam, E. (2004) Method validation for detection and quantification of cocoa butter equivalents in cocoa butter and plain chocolate. Journal of AOAC International 87, 1164-1172  

Buchgraber, M., Senaldi, C., Ulberth, F., Anklam, E. (2004) Detection and quantification of cocoa butter equivalents in cocoa butter and plain chocolate by gas liquid chromatography of triacylglycerols. Journal of AOAC International 87, 1153-1163

Buchgraber, M., Ulberth, F., Anklam, E. (2004) Cluster analysis for the systematic grouping of genuine cocoa butter and cocoa butter equivalent samples based on triglyceride patterns. Journal of Agricultural and Food Chemistry 52, 3855-3860

Ulberth, F., Buchgraber, M. (2003) Analytical platforms to assess the authenticity of cocoa butter.  European Journal of Lipid Science and Technology 105, 32-42

Brescia, M.A., Di Martino, G., Guillou, C., Reniero, F., Sacco, A., Serra, F. (2002) Differentiation of the geographical origin of durum wheat semolina samples on the basis of isotopic composition. Rapid Communications in Mass Spectrometry 16, 2286-2290

Aleu, J., Fronza, G., Fuganti, C., Serra, S., Fauhl, C., Guillou, C., Reniero, F. (2002) Differentiation of natural and synthetic phenylacetic acids by 2H NMR of the derived benzoic acids. European Food Research and Technology 214, 63-66

Barcarolo, R., Anklam, E. (2002) Investigation of a threshold for a limit of detection of individual vegetable fats in mixtures with cocoa butter. Deutsche Lebensmittel-Rundschau 98, 44-49

Barcarolo, R., Anklam, E. (2001) Development of a rapid method for the detection of cocoa butter equivalents in mixtures with cocoa butter. Journal of AOAC International 84, 1485-1489

Fronza, G., Fuganti, C., Serra, S., Burke, A., Guillou, C., Reniero, F. (2001) The positional δ(18O) values of extracted and synthetic vanillin. Helvetica Chimica Acta 84, 351-359

Fronza, G., Fuganti, C., Grasselli, P., Serra, S., Reniero, F., Guillou, C., Rossmann, A. (2001) δ13C- and δ18O-values of glycerol of food fats. Rapid Communications in Mass Spectrometry 15, 763-766

Lipp, M., Simoneau, C., Ulberth, F., Anklam, E., Crew, C., Brereton, P., de Greyt, W., Schwack, W., Wiedmaier, C. (2001) Composition of genuine cocoa butter and cocoa butter equivalents. Journal of Food Composition and Analysis 14, 399-408

Radovic, B.S., Careri, M., Mangia, A., Musci, M., Gerboles, M., Anklam, E. (2001) Contribution of dynamic headspace GC-MS analysis of aroma compounds to authenticity testing of honey. Food Chemistry 72, 511-520

Contarini, G., Povolo, M., Toppino, P.M., Radovic, B., Lipp, M., Anklam, E. (2001) Comparison of three different techniques for the discrimination of cheese: Application to the ewe's cheese. Milchwissenschaft 56, 136-140

Radovic, B.S., White, R., Parker, I., Dennis, M.J., Sharman, M., Geiss, H., Anklam, E. (2001) Contribution of high temperature gas chromatographic analysis of oligosaccharides and ion chromatographic analysis of various cations and anions to authenticity testing of honey. Deutsche Lebensmittel-Rundschau 97, 380-384

Tomás-Barberán, F.A., Martos, I., Ferreres, F., Radovic, B.S., Anklam, E. (2001) HPLC flavonoid profiles as markers for the botanical origin of European unifloral honeys.  Journal of the Science of Food and Agriculture 81, 485-496

Goodacre, R., Anklam, E. (2001) Fourier transform infrared spectroscopy and chemometrics as a tool for the rapid detection of other vegetable fats mixed in cocoa butter.  JAOCS, Journal of the American Oil Chemists' Society 78, 993-1000

Simoneau, C., Lipp, M., Ulberth, F., Anklam, E. (2000) Quantification of cocoa butter equivalents in mixtures with cocoa butter by chromatographic methods and multivariate data evaluation. European Food Research and Technology 211, 147-152

Buchgraber, M., Ulberth, F., Anklam, E. (2000) Comparison of HPLC and GLC techniques for the determination of the triglyceride profile of cocoa butter. Journal of Agricultural and Food Chemistry 48, 3359-3363

Ulberth, F., Buchgraber, M. (2000) Authenticity of fats and oils. European Journal of Lipid Science and Technology 102, 687-694

Sacco, A., Brescia, M.A., Liuzzi, V., Reniero, F., Guillou, C., Ghelli, S., Van Der Meer, P. (2000) Characterization of Italian olive oils based on analytical and nuclear magnetic resonance determinations.  JAOCS, Journal of the American Oil Chemists' Society 77, 619-625  

Book chapters:
Ulberth, F. (2016) Advances in testing for adulteration in honey. In Advances in Food Authenticity Testing (edited by G. Downey), Woodhead Publishing Series in Food Science, Technology and Nutrition, pp. 729-745

Kelly, S., Brereton, P., Guillou, C., Broll, H., Laube, I., Downey, G., Rossman, A., Hözl, S., van der Veer, G. (2011) New approaches to determining the origin of food. In Food chain integrity: A holistic approach to food traceability, safety, quality and authenticity (edited by J. Hoorfar, K.N. Jordan, F. Butler, R. Prugger), Woodhead Publishing Limited, pp. 238-258

Alonso-Salces, R.M., Moreno-Rojas, J.M., Holland, M.V., Guillou, C. (2010) Authentication of virgin olive oil by 1H-NMR and δ13C and δ2H-IRMS. In Olive Oil and Health (edited by J.D. Corrigan), Nova Science Publishers, Inc, pp. 73-110

Alonso-Salces, R.M., Serra, F., Reniero, F., Guillou, C. (2007) Analytical methods for the profiling of intrinsic quality of green coffee: Varietal and geographical characterisation, in Rapid Methods: For Food and Feed Quality Determination (edited by A. Van Amerongen, D. Barug, M. Lauwaars), Wageningen Academic Publishers, pp. 197-216

Rezzi, S., Guillou, C., Reniero, F., Holland, V.M., Ghelli, S. (2004) Natural abundance 2H-NMR spectroscopy. Application to food analysis. In Handbook of Stable Isotope Analytical Techniques (edited by P.A. de Groot), Elsevier B.V., pp. 103-121

Ulberth, F. (2003) Milk and dairy products, in Food Authenticity and Traceability (edited by M. Lees), Woodhead Publishing Series in Food Science, Technology and Nutrition, pp. 357-377.

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